P.acaciicola (compound 26) (0.33Hz/8)


Gaussian numbering
1H-1H Js
 -ppm- -#-   H4    H16   H17   H20   H21   H22   H23   H24   H26   H27   H29   H30   H31   H32   H33   H34   H35   H36   H37   H38   
  1.94 H4 
  5.99 H16    - 
  6.33 H17    -   10.2
  1.94 H20    -     -     - 
  1.93 H21    -     -     -     - 
  1.57 H22    -     -     -     -  -14.1
  2.11 H23    -     -     -     -    1.5   6.6
  2.55 H24    -     -     -     -    6.4  13.8 -13.3
  3.59 H26    -     -     -     -     -     -    7.6  10.4
  3.96 H27    -     -     -     -     -     -    0.7    -    3.3
  2.50 H29    -     -     -     -    3.8    -    0.6    -     -    4.7
  1.23 H30    -     -     -     -     -     -     -     -     -    1.6 -13.3
  1.94 H31    -     -     -     -     -     -     -     -     -     -     -     - 
  1.01 H32    -     -     -     -     -     -     -     -     -     -     -     -     - 
  1.01 H33    -     -     -     -     -     -     -     -     -     -     -     -     -     - 
  1.89 H34    -     -     -     -     -     -     -     -    6.3    -     -     -     -     -     - 
  1.01 H35    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
  1.23 H36    -     -     -     -     -     -     -     -     -     -     -     -     -    0.7   0.7    -    0.7
  1.23 H37    -     -     -     -     -     -     -     -     -     -     -     -     -    0.7   0.7    -    0.7    - 
  1.23 H38    -     -     -     -     -     -     -     -     -     -     -     -     -    0.7   0.7    -    0.7    -     - 

13C-1H Js
 -ppm- -#-   H4    H16   H17   H20   H21   H22   H23   H24   H26   H27   H29   H30   H31   H32   H33   H34   H35   H36   H37   H38   
195.39 C2    3.8   0.9  11.2   3.8    -     -     -     -     -    1.5    -    0.7   3.8    -     -     -     -     -     -     - 
 88.31 C3   -3.7   4.3    -   -3.7   1.8   8.1    -     -     -   -0.7   1.5   6.2  -3.7    -     -     -     -     -     -     - 
 42.19 C5    2.7    -    5.8   2.7  -3.3  -3.7   6.3   0.6    -    4.4  -3.5  -3.9   2.7   3.0   3.0    -    3.0   3.1   3.1   3.1
 42.12 C6     -    8.6   2.9    -    1.5   2.0    -     -     -     -    1.6   1.7    -   -3.3  -3.3    -   -3.3  -3.3  -3.3  -3.3
156.37 C7     -   -1.2 158.4    -     -     -     -     -     -     -     -     -     -    4.8   4.8    -    4.8   4.1   4.1   4.1
126.82 C8     -  167.7  -0.9    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
 30.96 C9     -     -     -     -  130.7 126.4  -3.1  -4.8   0.6    -    7.4   2.4    -    0.8   0.8    -    0.8    -     -     - 
 22.85 C11 131.6    -     -  131.6    -    1.0    -     -     -     -     -     -  131.6    -     -     -     -     -     -     - 
 33.34 C12    -     -     -     -   -3.4  -4.7 129.2 137.3  -2.7   4.6    -     -     -     -     -     -     -     -     -     - 
 69.34 C13    -     -     -     -    8.6   1.1  -4.7  -6.0 141.0  -3.9   6.2   1.4    -     -     -     -     -     -     -     - 
 24.64 C14    -   -0.8   3.9    -     -     -     -     -     -     -     -     -     -  129.1 129.1    -  129.1   5.5   5.5   5.5
 21.99 C15   0.8  -1.1   1.8   0.8    -     -     -     -     -     -     -     -    0.8   5.2   5.2    -    5.2 129.0 129.0 129.0
 80.27 C18    -     -     -     -     -     -    5.6   1.0    -  150.0  -4.8  -2.0    -     -     -     -     -     -     -     - 
 27.23 C19    -     -    0.9    -    7.7   2.3    -     -    0.8  -2.9 132.8 127.9    -     -     -     -     -     -     -     - 
 -ppm- -#-   H4    H16   H17   H20   H21   H22   H23   H24   H26   H27   H29   H30   H31   H32   H33   H34   H35   H36   H37   H38   
1H data (JH-H abs sorted)

6.33 (10.2)
5.99 (10.2)
3.96 (4.7, 3.3, 1.6, 0.7)
3.59 (10.4, 7.6, 6.3, 3.3)
2.55 (13.8, 13.3, 10.4, 6.4)
2.50 (13.3, 4.7, 3.8, 0.6)
2.11 (13.3, 7.6, 6.6, 1.5)
1.94
1.93 (14.1, 6.4, 3.8, 1.5)
1.89 (6.3)
1.57 (14.1, 13.8, 6.6)
1.23 (13.3, 1.6)
1.23 (0.7, 0.7, 0.7)
1.01 (0.7, 0.7, 0.7)
13C data
  2 195.4 (11.2, 3.8, 3.8, 3.8)
  7 156.4 (158.4, 4.8, 4.8, 4.8)
  8 126.8 (167.7, -0.9)
  3  88.3 (8.1, 6.2, 4.3, -3.7)
 18  80.3 (150.0, 5.6, -4.8, -2.0)
 13  69.3 (141.0, 8.6, 6.2, -6.0)
  5  42.2 (6.3, 5.8, 4.4, -3.9)
  6  42.1 (8.6, -3.3, -3.3, -3.3)
 12  33.3 (137.3, 129.2, -4.7, 4.6)
  9  31.0 (130.7, 126.4, 7.4, -4.8)
 19  27.2 (132.8, 127.9, 7.7, -2.9)
 14  24.6 (129.1, 129.1, 129.1, 5.5)
 11  22.8 (131.6, 131.6, 131.6, 1.0)
 15  22.0 (129.0, 129.0, 129.0, 5.2)