pallambin A (0.22Hz/12)


Gaussian numbering
1H-1H Js
 -ppm- -#-   H1    H8    H12   H14   H17   H18   H19   H21   H22   H23   H24   H28   H29   H31   H33   H34   H35   H37   H38   H39   H44   H45   
  2.45 H1 
  1.24 H8     - 
  0.45 H12    -    8.1
  2.64 H14   1.0   1.1    - 
  1.27 H17    -     -     -     - 
  1.27 H18    -     -     -     -     - 
  1.27 H19    -     -     -     -     -     - 
  1.30 H21    -    3.2  -6.6    -     -     -     - 
  0.68 H22   1.5   6.2   7.5    -     -     -     -    3.5
  1.50 H23    -     -     -     -     -     -     -     -     - 
  1.50 H24    -     -     -     -     -     -     -     -     -     - 
  2.33 H28    -    0.7    -     -     -     -     -     -     -     -     - 
  1.50 H29    -     -     -     -     -     -     -     -     -     -     -     - 
  4.63 H31    -     -     -     -     -     -     -     -     -     -     -    7.3    - 
  1.03 H33    -     -     -     -     -     -     -     -     -     -     -     -     -     - 
  1.03 H34    -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
  1.03 H35    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
  4.61 H37    -     -     -     -     -     -     -     -     -     -     -     -     -    3.7    -     -     - 
  6.66 H38    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
  2.59 H39    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -    0.6   7.5
  2.59 H44    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -    0.6   7.5    - 
  2.59 H45    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -    0.6   7.5    -     - 

13C-1H Js
 -ppm- -#-   H1    H8    H12   H14   H17   H18   H19   H21   H22   H23   H24   H28   H29   H31   H33   H34   H35   H37   H38   H39   H44   H45   
 17.00 C2   -1.2  -2.2  -1.9   7.7    -     -     -   -2.9 170.3    -     -     -     -     -     -     -     -     -     -     -     -     - 
 59.60 C3  150.7   1.7   3.5   4.8    -     -     -    2.6   3.0   4.2   4.2   3.9   4.2    -     -     -     -     -     -     -     -     - 
214.15 C4   -2.3    -     -    6.3   4.6   4.6   4.6    -    1.9    -     -     -     -     -     -     -     -     -     -     -     -     - 
 69.13 C5    2.0   1.4    -   -1.9  -4.4  -4.4  -4.4    -     -     -     -    1.8    -     -    2.9   2.9   2.9    -     -     -     -     - 
 56.45 C6    7.0   2.0   4.4 149.6   3.6   3.6   3.6   3.2   2.4   3.1   3.1   6.1   3.1    -     -     -     -     -     -     -     -     - 
 47.48 C7     -    6.1    -   -2.0    -     -     -     -    5.9  -4.2  -4.2  -3.6  -4.2   1.1    -     -     -     -     -     -     -     - 
 90.51 C10    -     -    0.6   1.1   3.9   3.9   3.9    -     -     -     -   -0.8    -    3.3  -4.0  -4.0  -4.0    -     -     -     -     - 
 61.98 C11   0.9    -     -     -     -     -     -     -     -    4.1   4.1 134.9   4.1    -    3.8   3.8   3.8    -     -     -     -     - 
  6.35 C13    -     -     -    1.1 129.1 129.1 129.1    -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
 15.21 C15   6.4 167.1  -2.6    -     -     -     -   -2.6  -2.4    -     -     -     -     -     -     -     -     -     -     -     -     - 
 20.52 C16   1.7    -     -    1.8    -     -     -     -     -  130.1 130.1   0.9 130.1    -     -     -     -     -     -     -     -     - 
 12.19 C20    -   -1.2 151.2    -     -     -     -  163.8    -    1.3   1.3    -    1.3    -     -     -     -     -     -     -     -     - 
 16.96 C26    -     -     -     -     -     -     -     -     -     -     -    3.5    -     -  128.4 128.4 128.4    -     -     -     -     - 
 83.74 C27    -     -     -     -     -     -     -     -     -     -     -     -     -  157.7    -     -     -    3.2    -     -     -     - 
 79.97 C30    -     -     -     -     -     -     -     -     -     -     -    1.6    -    2.1    -     -     -  156.6   5.1  -0.6  -0.6  -0.6
127.68 C36    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -   -1.1  -0.6   5.8   5.8   5.8
149.96 C40    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -    2.9 156.2  -7.1  -7.1  -7.1
168.03 C41    -     -     -     -     -     -     -     -     -     -     -     -     -    1.3    -     -     -    5.8  13.8  -1.0  -1.0  -1.0
 14.58 C43    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -    1.4 130.8 130.8 130.8
 -ppm- -#-   H1    H8    H12   H14   H17   H18   H19   H21   H22   H23   H24   H28   H29   H31   H33   H34   H35   H37   H38   H39   H44   H45   
1H data (JH-H abs sorted)

6.66 (7.5, 7.5, 7.5)
4.63 (7.3, 3.7)
4.61 (3.7, 0.6, 0.6, 0.6)
2.64 (1.1, 1.0)
2.59 (7.5, 0.6)
2.45 (1.5, 1.0)
2.33 (7.3, 0.7)
1.50
1.30 (6.6, 3.5, 3.2)
1.27
1.24 (8.1, 6.2, 3.2, 1.1)
1.03
0.68 (7.5, 6.2, 3.5, 1.5)
0.45 (8.1, 7.5, 6.6)
13C data
  4 214.1 (6.3, 4.6, 4.6, 4.6)
 41 168.0 (13.8, 5.8, 1.3, -1.0)
 40 150.0 (156.2, -7.1, -7.1, -7.1)
 36 127.7 (5.8, 5.8, 5.8, -1.1)
 10  90.5 (-4.0, -4.0, -4.0, 3.9)
 27  83.7 (157.7, 3.2)
 30  80.0 (156.6, 5.1, 2.1, 1.6)
  5  69.1 (-4.4, -4.4, -4.4, 2.9)
 11  62.0 (134.9, 4.1, 4.1, 4.1)
  3  59.6 (150.7, 4.8, 4.2, 4.2)
  6  56.5 (149.6, 7.0, 6.1, 4.4)
  7  47.5 (6.1, 5.9, -4.2, -4.2)
 16  20.5 (130.1, 130.1, 130.1, 1.8)
  2  17.0 (170.3, 7.7, -2.9, -2.2)
 26  17.0 (128.4, 128.4, 128.4, 3.5)
 15  15.2 (167.1, 6.4, -2.6, -2.6)
 43  14.6 (130.8, 130.8, 130.8, 1.4)
 20  12.2 (163.8, 151.2, 1.3, 1.3)
 13   6.3 (129.1, 129.1, 129.1, 1.1)