paucidactine D (0.28Hz/11)


Gaussian numbering
1H-1H Js
 -ppm- -#-   H26   H27   H28   H29   H30   H31   H32   H33   H34   H35   H36   H37   H38   H39   H40   H41   H42   H43   H44   H45   
  6.80 H26
  7.15 H27   7.4
  6.62 H28   1.0   7.9
  6.98 H29   7.4   1.3   0.7
  2.72 H30    -     -     -     - 
  1.29 H31    -     -     -     -     - 
  2.11 H32    -     -     -     -     -  -13.3
  1.68 H33    -     -     -     -     -   12.0   6.6
  1.46 H34    -     -     -     -     -    3.4  12.2 -13.1
  3.71 H35    -     -     -     -     -     -     -     -     - 
  1.65 H36    -     -     -     -     -     -     -     -     -     - 
  1.53 H37    -     -     -     -     -     -     -     -     -     -  -13.6
  1.44 H38    -     -     -     -     -     -     -     -     -     -    2.6   4.4
  1.89 H39    -     -     -     -     -     -     -     -     -     -    4.0  13.9 -13.7
  2.80 H40    -     -     -     -     -     -     -     -     -     -     -     -    3.8  12.8
  4.42 H41    -     -     -     -     -     -     -     -     -     -    1.4    -    1.3   5.5 -12.8
  4.49 H42    -     -     -     -     -     -     -     -     -     -     -     -     -     -    1.2    - 
  2.81 H43    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
  2.20 H44    -     -     -     -     -     -     -     -    3.7    -     -     -     -     -     -     -     -    4.9
  1.56 H45    -     -     -     -     -     -     -     -     -    1.7    -     -     -     -     -     -     -   11.6 -15.2

13C-1H Js
 -ppm- -#-   H26   H27   H28   H29   H30   H31   H32   H33   H34   H35   H36   H37   H38   H39   H40   H41   H42   H43   H44   H45   
120.33 C1  163.6   1.3   6.9   0.6    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
129.80 C2    2.0 161.2    -    7.3    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
111.15 C3    8.2   1.5 160.8  -1.4    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
151.01 C4   -1.5   9.0  -0.7   8.2    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
133.91 C5    8.0  -1.5   5.8    -     -     -     -     -     -    4.4    -     -     -     -     -     -    5.0   0.8    -     - 
122.06 C6    2.0   8.5  -1.3 159.7    -     -     -     -     -     -     -     -     -     -     -     -     -     -     -     - 
 67.22 C8     -     -     -     -     -   -4.2  -4.4   1.6   2.8   0.6    -     -     -     -     -     -    1.4  -4.2   1.5   2.5
 48.82 C9     -     -     -    3.0    -    6.7   2.7    -     -   -3.3   1.0    -     -     -     -     -   -1.9   5.3    -     - 
 28.04 C10    -     -     -     -     -  130.0 133.1  -3.8  -3.5    -     -     -     -     -     -     -     -    3.1    -     - 
 32.91 C11    -     -     -     -     -   -3.9  -3.7 131.1 130.3   2.5   1.6   3.1    -     -     -     -     -     -    8.6   2.8
 33.92 C12    -     -     -     -     -    2.7   1.3  -3.7  -3.7    -   -4.0  -3.5   6.6   1.4    -     -     -    1.5  -3.6  -3.3
 65.20 C13    -     -     -     -     -     -     -   10.0   3.1 146.2   6.6   1.7    -     -    0.9   5.1   2.6    -    1.8   7.7
 34.30 C14    -     -     -     -     -     -     -    1.7   2.6   1.4 130.2 124.7  -3.7  -3.5   1.7   7.3    -     -    1.3   2.0
 20.47 C15    -     -     -     -     -     -     -     -     -     -   -3.6  -3.9 131.0 129.2  -2.2  -2.8    -     -     -     - 
 38.99 C16    -     -     -     -     -     -     -     -     -    0.8   8.1   2.1  -2.0  -4.3 136.6 144.9    -     -     -     - 
166.85 C18    -     -     -     -     -     -     -     -     -    4.5    -     -     -     -    4.1   2.6  -4.4    -     -     - 
 85.23 C19    -     -     -   -0.7    -     -     -     -     -    3.3    -     -     -     -     -     -  164.3   0.7    -     - 
 41.26 C20    -     -     -     -     -    3.5   6.6    -     -     -     -    0.9    -     -     -     -     -  141.7  -3.2  -3.6
 29.34 C21    -     -     -     -     -     -     -    3.2   7.8   4.7   2.4   7.2    -     -     -     -     -   -3.9 131.2 134.5
167.04 C22    -     -     -     -     -     -    1.9    -     -     -     -     -     -     -     -     -    4.7  -5.2   7.5   3.1
 -ppm- -#-   H26   H27   H28   H29   H30   H31   H32   H33   H34   H35   H36   H37   H38   H39   H40   H41   H42   H43   H44   H45   
1H data (JH-H abs sorted)

7.15 (7.9, 7.4, 1.3)
6.98 (7.4, 1.3, 0.7)
6.80 (7.4, 7.4, 1.0)
6.62 (7.9, 1.0, 0.7)
4.49 (1.2)
4.42 (12.8, 5.5, 1.4, 1.3)
3.71 (1.7)
2.81 (11.6, 4.9)
2.80 (12.8, 12.8, 3.8, 1.2)
2.72
2.20 (15.2, 4.9, 3.7)
2.11 (13.3, 12.2, 6.6)
1.89 (13.9, 13.7, 12.8, 4.0)
1.68 (13.1, 12.0, 6.6)
1.65 (13.6, 4.0, 2.6, 1.4)
1.56 (15.2, 11.6, 1.7)
1.53 (13.9, 13.6, 4.4)
1.46 (13.1, 12.2, 3.7, 3.4)
1.44 (13.7, 4.4, 3.8, 2.6)
1.29 (13.3, 12.0, 3.4)
13C data
 22 167.0 (7.5, -5.2, 4.7, 3.1)
 18 166.9 (4.5, -4.4, 4.1, 2.6)
  4 151.0 (9.0, 8.2, -1.5, -0.7)
  5 133.9 (8.0, 5.8, 5.0, 4.4)
  2 129.8 (161.2, 7.3, 2.0)
  6 122.1 (159.7, 8.5, 2.0, -1.3)
  1 120.3 (163.6, 6.9, 1.3, 0.6)
  3 111.1 (160.8, 8.2, 1.5, -1.4)
 19  85.2 (164.3, 3.3, -0.7, 0.7)
  8  67.2 (-4.4, -4.2, -4.2, 2.8)
 13  65.2 (146.2, 10.0, 7.7, 6.6)
  9  48.8 (6.7, 5.3, -3.3, 3.0)
 20  41.3 (141.7, 6.6, -3.6, 3.5)
 16  39.0 (144.9, 136.6, 8.1, -4.3)
 14  34.3 (130.2, 124.7, 7.3, -3.7)
 12  33.9 (6.6, -4.0, -3.7, -3.7)
 11  32.9 (131.1, 130.3, 8.6, -3.9)
 21  29.3 (134.5, 131.2, 7.8, 7.2)
 10  28.0 (133.1, 130.0, -3.8, -3.5)
 15  20.5 (131.0, 129.2, -3.9, -3.6)